Journal of Microwave Power and Electromagnetic Energy (JMPEE)

 

TITLE

A New Microwave Reactor Suitable for Organic Synthesis and Kinetics Studies [PDF]

AUTHORS

D. Constable, K. Raner, P. Somlo and C. Strauss

1992

27

4

195-198

YEAR

VOLUME

ISSUE

PAGES

 

Abstract

A microwave unit and reaction vessel for chemical synthesis or kinetics studies is described. The Teflon reaction vessel could be operated at temperatures up to 200 °C and pressures up to 10 atmospheres. It was possible to stir and directly monitor the temperature and pressure in the microwave environment. The system was demonstrated by preparing isopropyl 2,4, 6-trimethylbenzoate.

 

Key Words:

Microwave, Chemical synthesis, Chemical reactor, Kinetics, Temperature monitoring, Magnetic stirring.